Evaluation of Fracture Toughness of γ-Phase Containing Cemented Carbides by Using Through-Thickness Micronotches Shaped by Ultrashort Pulsed Laser Ablation

Abstract

[EN]WC-Co cemented carbides, commonly known as hardmetals, are composite materials constituted by hard ceramic particles embedded in a ductile metal matrix. Due to their unique microstructural assemblage, these materials exhibit excellent combinations of hardness, strength, and toughness, consolidating them as a first choice for tools, structural and wear components. During recent decades, extensive research and technological advancements have driven the development of alternative cemented carbide grades, where traditionally used WC or Co are partially or entirely replaced. Within this context, hardmetals containing a third γ-phase (mixed cubic carbides) represent an interesting alternative. However, accurate evaluation of their fracture toughness remains a significant issue, especially as conventional methods using either indentation or precracking approaches are limited by either restricted implementation of fracture mechanics analysis or testing challenges. Within this context, this study proposes, implements, and validates the use of a novel laser-micronotching methodology to evaluate the fracture toughness of a γ-phase containing cemented carbide grade. For comparison purposes, the investigation also includes assessment of such a property by means of two other well-established testing methodologies. Moreover, similar experimental work was conducted in a plain WC-Co system with similar microstructural features. It is shown that machining of a through-thickness micronotch by means of ultra-short pulsed laser ablation is a reliable and efficient method for fracture toughness evaluation of γ-phase containing hardmetals. The main reason behind this is its capability for providing a precise and reproducible micronotch, with minimal thermal damage, that finally acts as a real through-thickness crack for which a stress-intensity factor is well-defined under flexural testing. Furthermore, toughness values obtained are in satisfactory agreement with those determined using precracked specimens with machined large notches and/or indentation techniques.